| Id |
Subject |
Object |
Predicate |
Lexical cue |
| TextSentencer_T1 |
0-91 |
Sentence |
denotes |
X-ray crystal structure of galabiose, O-alpha-D-galactopyranosyl-(1---4)-D-galactopyranose. |
| T1 |
0-91 |
Sentence |
denotes |
X-ray crystal structure of galabiose, O-alpha-D-galactopyranosyl-(1---4)-D-galactopyranose. |
| TextSentencer_T2 |
92-317 |
Sentence |
denotes |
O-alpha-D-Galactopyranosyl-(1---4)-D-galactopyranose, C12H22O11, Mr = 342.30, crystallises in the orthorhombic space group P2(1)2(1)2(1), and has alpha = 5.826(1), b = 13.904(3), c = 17.772(4) A, Z = 4, and Dx = 1.579 g.cm-3. |
| T2 |
92-317 |
Sentence |
denotes |
O-alpha-D-Galactopyranosyl-(1---4)-D-galactopyranose, C12H22O11, Mr = 342.30, crystallises in the orthorhombic space group P2(1)2(1)2(1), and has alpha = 5.826(1), b = 13.904(3), c = 17.772(4) A, Z = 4, and Dx = 1.579 g.cm-3. |
| TextSentencer_T3 |
318-375 |
Sentence |
denotes |
Intensity data were collected with a CAD4 diffractometer. |
| T3 |
318-375 |
Sentence |
denotes |
Intensity data were collected with a CAD4 diffractometer. |
| TextSentencer_T4 |
376-492 |
Sentence |
denotes |
The structure was solved by direct methods and refined to R = 0.063 and Rw = 0.084 for 2758 independent reflections. |
| T4 |
376-492 |
Sentence |
denotes |
The structure was solved by direct methods and refined to R = 0.063 and Rw = 0.084 for 2758 independent reflections. |
| TextSentencer_T5 |
493-749 |
Sentence |
denotes |
The glycosidic linkage is of the type 1-axial-4-axial with torsion angles phi O-5' (O-5'-C-1'-O-1'-C-4) = 98.1(2) degrees, psi C-3 (C-3-C-4-O-1'-C-1') = -81.9(3) degrees, phi H (H-1'-C-1'-O-1'-C-4) = -18 degrees, and psi H (H-4-C-4-O-1'-C-1') = 35 degrees. |
| T5 |
493-749 |
Sentence |
denotes |
The glycosidic linkage is of the type 1-axial-4-axial with torsion angles phi O-5' (O-5'-C-1'-O-1'-C-4) = 98.1(2) degrees, psi C-3 (C-3-C-4-O-1'-C-1') = -81.9(3) degrees, phi H (H-1'-C-1'-O-1'-C-4) = -18 degrees, and psi H (H-4-C-4-O-1'-C-1') = 35 degrees. |
| TextSentencer_T6 |
750-796 |
Sentence |
denotes |
The conformation is stabilised by an O-3 . . . |
| T6 |
750-796 |
Sentence |
denotes |
The conformation is stabilised by an O-3 . . . |
| TextSentencer_T7 |
797-869 |
Sentence |
denotes |
O-5' intramolecular hydrogen-bond with length 2.787(3) A and O-3-H . . . |
| T7 |
797-869 |
Sentence |
denotes |
O-5' intramolecular hydrogen-bond with length 2.787(3) A and O-3-H . . . |
| TextSentencer_T8 |
870-889 |
Sentence |
denotes |
O-5' = 162 degrees. |
| T8 |
870-889 |
Sentence |
denotes |
O-5' = 162 degrees. |
| TextSentencer_T9 |
890-1037 |
Sentence |
denotes |
The glycosidic linkage causes a folding of the molecule with an angle of 117 degrees between the least-square planes through the pyranosidic rings. |
| T9 |
890-1037 |
Sentence |
denotes |
The glycosidic linkage causes a folding of the molecule with an angle of 117 degrees between the least-square planes through the pyranosidic rings. |
| TextSentencer_T10 |
1038-1269 |
Sentence |
denotes |
The crystal investigated contained 56(1)% of alpha- and 44(1)% of beta-galabiose as well as approximately 70% of the gauche-trans and approximately 30% of the trans-gauche conformers about the exocyclic C-5'-C-6' and C-5-C-6 bonds. |
| T10 |
1038-1269 |
Sentence |
denotes |
The crystal investigated contained 56(1)% of alpha- and 44(1)% of beta-galabiose as well as approximately 70% of the gauche-trans and approximately 30% of the trans-gauche conformers about the exocyclic C-5'-C-6' and C-5-C-6 bonds. |
| TextSentencer_T11 |
1270-1429 |
Sentence |
denotes |
The crystal packing is governed by hydrogen bonding that engages all oxygen atoms except the intramolecular acceptor O-5' and the glycosidic O-1' oxygen atoms. |
| T11 |
1270-1429 |
Sentence |
denotes |
The crystal packing is governed by hydrogen bonding that engages all oxygen atoms except the intramolecular acceptor O-5' and the glycosidic O-1' oxygen atoms. |
