| Id |
Subject |
Object |
Predicate |
Lexical cue |
| TextSentencer_T1 |
0-167 |
Sentence |
denotes |
Acid-catalyzed dehydrative cyclization of 4-(D-galacto -pentitol-1-yl)-2-phenyl-2H-1,2,3-triazole. synthesis and anomeric configuration of D-lyxo-C-nucleoside analogs. |
| T1 |
0-167 |
Sentence |
denotes |
Acid-catalyzed dehydrative cyclization of 4-(D-galacto -pentitol-1-yl)-2-phenyl-2H-1,2,3-triazole. synthesis and anomeric configuration of D-lyxo-C-nucleoside analogs. |
| TextSentencer_T2 |
168-483 |
Sentence |
denotes |
Dehydration of 4-(D-galacto-pentitol-1-yl)-2-phenyl-2H-1,2,3-triazole with 20% methanolic sulfuric acid afforded the anomeric pairs of nucleosides, 4-(alpha-D-lyxopyranosyl)-2-phenyl-2H-1,2,3-triazole (major component) and its beta-anomer, as well as 4-(alpha-D-lyxofuranosyl)-2H-1,2,3-triazole and its beta-anomer. |
| T2 |
168-483 |
Sentence |
denotes |
Dehydration of 4-(D-galacto-pentitol-1-yl)-2-phenyl-2H-1,2,3-triazole with 20% methanolic sulfuric acid afforded the anomeric pairs of nucleosides, 4-(alpha-D-lyxopyranosyl)-2-phenyl-2H-1,2,3-triazole (major component) and its beta-anomer, as well as 4-(alpha-D-lyxofuranosyl)-2H-1,2,3-triazole and its beta-anomer. |
| TextSentencer_T3 |
484-698 |
Sentence |
denotes |
The four anomeric C-nucleosides were separated by chromatography, and their structure and anomeric configuration were determined by periodate oxidation, acylation, and NMR spectroscopy as well as mass spectrometry. |
| T3 |
484-698 |
Sentence |
denotes |
The four anomeric C-nucleosides were separated by chromatography, and their structure and anomeric configuration were determined by periodate oxidation, acylation, and NMR spectroscopy as well as mass spectrometry. |
| TextSentencer_T4 |
699-858 |
Sentence |
denotes |
The anomeric assignment from optical rotation was not in agreement with final structure assignment and represented a violation of the Hudson isorotation rules. |
| T4 |
699-858 |
Sentence |
denotes |
The anomeric assignment from optical rotation was not in agreement with final structure assignment and represented a violation of the Hudson isorotation rules. |
| TextSentencer_T5 |
859-943 |
Sentence |
denotes |
NOE studies and X-ray diffraction measurements confirmed the anomeric configuration. |
| T5 |
859-943 |
Sentence |
denotes |
NOE studies and X-ray diffraction measurements confirmed the anomeric configuration. |