| Id |
Subject |
Object |
Predicate |
Lexical cue |
| T274 |
0-52 |
Sentence |
denotes |
To a solution of 18 or 26–29 in anhydrous DMF (conc. |
| T275 |
53-131 |
Sentence |
denotes |
0.13 M) was successively added 17 (1.10 eq), KI (0.30 eq) and K2CO3 (3.00 eq). |
| T276 |
132-222 |
Sentence |
denotes |
After stirring for 24 h at 50 °C under argon, the reaction was diluted in AcOEt and water. |
| T277 |
223-372 |
Sentence |
denotes |
The aqueous layer was extracted with AcOEt and the combined organic extracts were washed with brine, dried over Na2SO4 and concentrated under vacuum. |
| T278 |
373-522 |
Sentence |
denotes |
The residue was purified by flash column chromatography (silica gel, linear gradient 0–8% MeOH in DCM) to give the desired compound as colored solid. |
