PMC:7291971 / 53618-54407
Annnotations
LitCovid-PMC-OGER-BB
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T1102 | 85-97 | CHEBI:38472;CHEBI:38472 | denotes | acetonitrile |
T1103 | 261-265 | CHEBI:51231;CHEBI:51231 | denotes | DMSO |
T86511 | 85-97 | CHEBI:38472;CHEBI:38472 | denotes | acetonitrile |
T14604 | 261-265 | CHEBI:51231;CHEBI:51231 | denotes | DMSO |
LitCovid-PubTator
Id | Subject | Object | Predicate | Lexical cue | tao:has_database_id |
---|---|---|---|---|---|
919 | 342-344 | Chemical | denotes | 2H | MESH:D003903 |
LitCovid-PD-CLO
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T335 | 58-59 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
T336 | 175-176 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
LitCovid-PD-CHEBI
Id | Subject | Object | Predicate | Lexical cue | chebi_id |
---|---|---|---|---|---|
T17575 | 85-97 | Chemical | denotes | acetonitrile | http://purl.obolibrary.org/obo/CHEBI_38472 |
T86424 | 107-113 | Chemical | denotes | buffer | http://purl.obolibrary.org/obo/CHEBI_35225 |
T108 | 244-246 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T24815 | 261-265 | Chemical | denotes | DMSO | http://purl.obolibrary.org/obo/CHEBI_28262 |
T20156 | 282-284 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T65687 | 296-298 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T8029 | 310-312 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T2651 | 324-326 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T5457 | 386-388 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T115 | 412-414 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T28173 | 457-459 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T85971 | 483-485 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T74956 | 515-517 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T36399 | 547-549 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T49547 | 573-575 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T89992 | 644-646 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
LitCovid-sentences
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T381 | 0-789 | Sentence | denotes | Following method C with 23 (40 mg, 0.45 mol, 1.00 eq) and a 0–50% linear gradient of acetonitrile in TEAAc buffer 50 mM, pH 7 for purification, 5 (20 mg, 72%) was obtained as a white powder with 98% purity determined by HPLC analysis at 260 nm.1H NMR (500 MHz, DMSO‑d 6) δ 8.36 (s, 1H), 8.32 (s, 1H), 8.14 (s, 1H), 8.13 (s, 1H), 7.33 (br. s, 2H), 7.25 (br. s, 2H), 5.97 (d, J = 6.3 Hz, 1H), 5.85 (d, J = 5.2 Hz, 1H), 5.49–5.39 (m, 3H), 5.14 (d, J = 5.3 Hz, 1H), 4.62 (q, J = 5.4 Hz, 1H), 4.52 (dd, J = 6.5, 4.7 Hz, 1H), 4.29 (dd, J = 4.8, 2.8 Hz, 1H), 4.06 (q, J = 4.9 Hz, 1H), 4.00–3.92 (m, 2H), 3.68–3.46 (m, 4H), 2.79 (dd, J = 14.0, 4.6 Hz, 1H), 2.70–2.51 (m, 3H), 2.41–2.30 (m, 2H), 1.22 (q, J = 7.4, 2H), 1.07 (tdd, J = 13.4 Hz, J = 10.5 Hz, J = 6.3 Hz, 2H), 0.73 (t, J = 7.3 Hz, 2H). |