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PMC:7291971 / 47354-47874 JSONTXT

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LitCovid-PMC-OGER-BB

Id Subject Object Predicate Lexical cue
T978 55-60 CHEBI:15377;CHEBI:15377 denotes water
T979 115-123 CHEBI:46787;CHEBI:46787 denotes solvents
T980 174-177 CHEBI:62946;CHEBI:62946 denotes NH3
T981 181-185 CHEBI:32145;CHEBI:32145 denotes MeOH
T982 229-237 CHEBI:46787;CHEBI:46787 denotes solvents
T983 331-337 CHEBI:30563;CHEBI:30563 denotes silica
T984 398-410 CHEBI:38472;CHEBI:38472 denotes acetonitrile
T985 474-482 CHEBI:36357;CHEBI:36357 denotes compound
T67269 55-60 CHEBI:15377;CHEBI:15377 denotes water
T97010 115-123 CHEBI:46787;CHEBI:46787 denotes solvents
T83843 174-177 CHEBI:62946;CHEBI:62946 denotes NH3
T7244 181-185 CHEBI:32145;CHEBI:32145 denotes MeOH
T36733 229-237 CHEBI:46787;CHEBI:46787 denotes solvents
T77353 331-337 CHEBI:30563;CHEBI:30563 denotes silica
T73055 398-410 CHEBI:38472;CHEBI:38472 denotes acetonitrile
T11993 474-482 CHEBI:36357;CHEBI:36357 denotes compound

LitCovid-PubTator

Id Subject Object Predicate Lexical cue tao:has_database_id
830 38-41 Chemical denotes TFA MESH:D014269
831 55-60 Chemical denotes water MESH:D014867
832 174-177 Chemical denotes NH3
833 181-185 Chemical denotes MeOH
834 331-341 Chemical denotes silica gel MESH:D058428
835 398-410 Chemical denotes acetonitrile MESH:C032159
836 414-419 Chemical denotes TEAAc

LitCovid-PD-CLO

Id Subject Object Predicate Lexical cue
T320 314-315 http://purl.obolibrary.org/obo/CLO_0001020 denotes a
T321 371-372 http://purl.obolibrary.org/obo/CLO_0001020 denotes a

LitCovid-PD-CHEBI

Id Subject Object Predicate Lexical cue chebi_id
T889 38-41 Chemical denotes TFA http://purl.obolibrary.org/obo/CHEBI_45892
T890 55-60 Chemical denotes water http://purl.obolibrary.org/obo/CHEBI_15377
T891 115-123 Chemical denotes solvents http://purl.obolibrary.org/obo/CHEBI_46787
T892 174-177 Chemical denotes NH3 http://purl.obolibrary.org/obo/CHEBI_16134
T893 181-185 Chemical denotes MeOH http://purl.obolibrary.org/obo/CHEBI_17790
T894 229-237 Chemical denotes solvents http://purl.obolibrary.org/obo/CHEBI_46787
T895 331-337 Chemical denotes silica http://purl.obolibrary.org/obo/CHEBI_30563
T896 398-410 Chemical denotes acetonitrile http://purl.obolibrary.org/obo/CHEBI_38472
T897 420-426 Chemical denotes buffer http://purl.obolibrary.org/obo/CHEBI_35225

LitCovid-sentences

Id Subject Object Predicate Lexical cue
T344 111-194 Sentence denotes The solvents were removed and the residue was treated with 7 M NH3 in MeOH (10 mL).
T345 195-439 Sentence denotes After stirring for 24 h at 30 °C, solvents were removed and the residue was purified by flash column chromatography on a reversed-phase silica gel column C18 (4 g, 40 μm) with a 0–15% linear gradient of acetonitrile in TEAAc buffer 50 mM, pH 7.