| Id |
Subject |
Object |
Predicate |
Lexical cue |
| TextSentencer_T1 |
0-92 |
Sentence |
denotes |
Purification of endo-N-acetyl-beta-D-glucosaminidase H by substrate-affinity chromatography. |
| TextSentencer_T2 |
93-230 |
Sentence |
denotes |
Endo-N-acetyl-beta-D-glucosaminidase H (Endo H) was purified to homogeneity (3000-fold) from a culture filtrate to Streptomyces plicatus. |
| TextSentencer_T3 |
231-393 |
Sentence |
denotes |
The key step was substrate-affinity chromatography, which afforded a 1000-fold purification and yielded a protease- and exoglycosidase-free preparation of Endo H. |
| TextSentencer_T4 |
394-562 |
Sentence |
denotes |
Proteins from the crude sample were applied to the substrate-affinity column, consisting of yeast-invertase glycopeptides bound to Sepharose-immobilized concanavalin A. |
| TextSentencer_T5 |
563-670 |
Sentence |
denotes |
After washing off the unbound proteins, Endo H was quantitatively eluted by methyl alpha-D-mannopyranoside. |
| TextSentencer_T6 |
671-773 |
Sentence |
denotes |
Various conditions were tested to achieve an optimal binding of Endo H to this substrate-affinity gel. |
| TextSentencer_T7 |
774-954 |
Sentence |
denotes |
After substrate-affinity chromatography, Endo H was separated from the coeluted gylcopeptide substrate and some protein impurities by gel filtration and hydrophobic chromatography. |
| T1 |
0-92 |
Sentence |
denotes |
Purification of endo-N-acetyl-beta-D-glucosaminidase H by substrate-affinity chromatography. |
| T2 |
93-230 |
Sentence |
denotes |
Endo-N-acetyl-beta-D-glucosaminidase H (Endo H) was purified to homogeneity (3000-fold) from a culture filtrate to Streptomyces plicatus. |
| T3 |
231-393 |
Sentence |
denotes |
The key step was substrate-affinity chromatography, which afforded a 1000-fold purification and yielded a protease- and exoglycosidase-free preparation of Endo H. |
| T4 |
394-562 |
Sentence |
denotes |
Proteins from the crude sample were applied to the substrate-affinity column, consisting of yeast-invertase glycopeptides bound to Sepharose-immobilized concanavalin A. |
| T5 |
563-670 |
Sentence |
denotes |
After washing off the unbound proteins, Endo H was quantitatively eluted by methyl alpha-D-mannopyranoside. |
| T6 |
671-773 |
Sentence |
denotes |
Various conditions were tested to achieve an optimal binding of Endo H to this substrate-affinity gel. |
| T7 |
774-954 |
Sentence |
denotes |
After substrate-affinity chromatography, Endo H was separated from the coeluted gylcopeptide substrate and some protein impurities by gel filtration and hydrophobic chromatography. |