PubMed:1816921 JSONTXT

{"project":"GlyCosmos600-Glycan-Motif-Structure","denotations":[{"id":"T1","span":{"begin":35,"end":44},"obj":"https://glytoucan.org/Structures/Glycans/G95090DW"},{"id":"T2","span":{"begin":35,"end":44},"obj":"https://glytoucan.org/Structures/Glycans/G72548RZ"},{"id":"T3","span":{"begin":35,"end":44},"obj":"https://glytoucan.org/Structures/Glycans/G40843KY"},{"id":"T4","span":{"begin":88,"end":97},"obj":"https://glytoucan.org/Structures/Glycans/G95090DW"},{"id":"T5","span":{"begin":88,"end":97},"obj":"https://glytoucan.org/Structures/Glycans/G72548RZ"},{"id":"T6","span":{"begin":88,"end":97},"obj":"https://glytoucan.org/Structures/Glycans/G40843KY"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"GlyCosmos6-Glycan-Motif-Image","denotations":[{"id":"T1","span":{"begin":35,"end":44},"obj":"Glycan_Motif"},{"id":"T4","span":{"begin":88,"end":97},"obj":"Glycan_Motif"}],"attributes":[{"id":"A1","pred":"image","subj":"T1","obj":"https://api.glycosmos.org/wurcs2image/0.10.0/png/binary/G95090DW"},{"id":"A2","pred":"image","subj":"T1","obj":"https://api.glycosmos.org/wurcs2image/0.10.0/png/binary/G72548RZ"},{"id":"A3","pred":"image","subj":"T1","obj":"https://api.glycosmos.org/wurcs2image/0.10.0/png/binary/G40843KY"},{"id":"A4","pred":"image","subj":"T4","obj":"https://api.glycosmos.org/wurcs2image/0.10.0/png/binary/G95090DW"},{"id":"A5","pred":"image","subj":"T4","obj":"https://api.glycosmos.org/wurcs2image/0.10.0/png/binary/G72548RZ"},{"id":"A6","pred":"image","subj":"T4","obj":"https://api.glycosmos.org/wurcs2image/0.10.0/png/binary/G40843KY"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"GlyCosmos6-Glycan-Motif-Structure","denotations":[{"id":"T1","span":{"begin":35,"end":44},"obj":"https://glytoucan.org/Structures/Glycans/G40843KY"},{"id":"T2","span":{"begin":35,"end":44},"obj":"https://glytoucan.org/Structures/Glycans/G72548RZ"},{"id":"T3","span":{"begin":35,"end":44},"obj":"https://glytoucan.org/Structures/Glycans/G95090DW"},{"id":"T4","span":{"begin":88,"end":97},"obj":"https://glytoucan.org/Structures/Glycans/G40843KY"},{"id":"T5","span":{"begin":88,"end":97},"obj":"https://glytoucan.org/Structures/Glycans/G72548RZ"},{"id":"T6","span":{"begin":88,"end":97},"obj":"https://glytoucan.org/Structures/Glycans/G95090DW"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"GlyCosmos600-FMA","denotations":[{"id":"T1","span":{"begin":374,"end":384},"obj":"Body_part"},{"id":"T2","span":{"begin":883,"end":893},"obj":"Body_part"}],"attributes":[{"id":"A1","pred":"fma_id","subj":"T1","obj":"http://purl.org/sig/ont/fma/fma82738"},{"id":"A2","pred":"fma_id","subj":"T2","obj":"http://purl.org/sig/ont/fma/fma82738"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"sentences","denotations":[{"id":"TextSentencer_T1","span":{"begin":0,"end":72},"obj":"Sentence"},{"id":"TextSentencer_T2","span":{"begin":73,"end":239},"obj":"Sentence"},{"id":"TextSentencer_T3","span":{"begin":240,"end":407},"obj":"Sentence"},{"id":"TextSentencer_T4","span":{"begin":408,"end":532},"obj":"Sentence"},{"id":"TextSentencer_T5","span":{"begin":533,"end":624},"obj":"Sentence"},{"id":"TextSentencer_T6","span":{"begin":625,"end":760},"obj":"Sentence"},{"id":"TextSentencer_T7","span":{"begin":761,"end":955},"obj":"Sentence"},{"id":"T1","span":{"begin":0,"end":72},"obj":"Sentence"},{"id":"T2","span":{"begin":73,"end":239},"obj":"Sentence"},{"id":"T3","span":{"begin":240,"end":407},"obj":"Sentence"},{"id":"T4","span":{"begin":408,"end":532},"obj":"Sentence"},{"id":"T5","span":{"begin":533,"end":624},"obj":"Sentence"},{"id":"T6","span":{"begin":625,"end":760},"obj":"Sentence"},{"id":"T7","span":{"begin":761,"end":955},"obj":"Sentence"}],"namespaces":[{"prefix":"_base","uri":"http://pubannotation.org/ontology/tao.owl#"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"glycosmos-test-glycan-structure","denotations":[{"id":"PD-GlycanStructures-B_T1","span":{"begin":35,"end":44},"obj":"http://rdf.glyconavi.org/CarTNa/CarTNa22/trivialname"},{"id":"PD-GlycanStructures-B_T2","span":{"begin":88,"end":97},"obj":"http://rdf.glyconavi.org/CarTNa/CarTNa22/trivialname"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"glycosmos-test-structure-v1","denotations":[{"id":"PD-GlycanStructures-B_T1","span":{"begin":35,"end":44},"obj":"http://rdf.glyconavi.org/CarTNa/CarTNa22/trivialname"},{"id":"PD-GlycanStructures-B_T2","span":{"begin":88,"end":97},"obj":"http://rdf.glyconavi.org/CarTNa/CarTNa22/trivialname"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

{"project":"GlyCosmos600-GlycoEpitope","denotations":[{"id":"PD-GlycoEpitope-B_T1","span":{"begin":522,"end":525},"obj":"http://www.glycoepitope.jp/epitopes/AN0578"}],"text":"Fast-atom-bombardment chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}

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chemistry of sulfatide (3-sulfogalactosylceramide)\nF.a.b.-m.s. of sulfatide (3-sulfogalactosylceramide, 1) in the negative-ion mode reveals the molecular weight and the presence of the sulfate ester without ambiguity. The size of the long-chain base is represented as the (M - H)- ion of the corresponding lyso-form (deacylated molecule) only when the fatty acid is alpha-hydroxylated. The spectrum in the positive-ion mode indicates the molecular weight by a pair of sodium adduct ions separated by 102 a.m.u. However, the desulfated fragment ion is not shown in the B/E-constant linked-scanning mode. If the long-chain base ion [CH2C(NH2) = CHR]+ is present, B/E-constant linked scanning confirms that the double bond is located at C-4. B/E-Constant linked scanning of the (M - H)- ions in the negative-ion mode indicates the location of a double bond in the fatty acid moiety at C-15 for the most abundant molecular species c24:1."}