| Id |
Subject |
Object |
Predicate |
Lexical cue |
| TextSentencer_T1 |
0-141 |
Sentence |
denotes |
Chlorination of cellulose with N-chlorosuccinimide-triphenylphosphine under homogeneous conditions in lithium chloride-N,N-dimethylacetamide. |
| TextSentencer_T2 |
142-288 |
Sentence |
denotes |
Microcrystalline cellulose was chlorinated with N-chlorosuccinimide-triphenylphosphine under homogeneous conditions in LiCl-N,N-dimethylacetamide. |
| TextSentencer_T3 |
289-468 |
Sentence |
denotes |
At the early stage of the reaction only replacement of the 6-hydroxyl groups with chlorine was observed, and 3-hydroxyl groups were replaced at a lower rate with Walden inversion. |
| TextSentencer_T4 |
469-557 |
Sentence |
denotes |
The effects of reaction conditions on the extent of chlorination were studied in detail. |
| TextSentencer_T5 |
558-739 |
Sentence |
denotes |
More than two equivalents of chlorination reagents per glucose residue were necessary to attain a high degree of substitution (ds) by chlorine, and the maximum ds attained was 1.86. |
| TextSentencer_T6 |
740-911 |
Sentence |
denotes |
Chlorinated disaccharides were found in the hydrolyzates of chlorodeoxycelluloses hydrolyzed under mild conditions, and their structures were studied by mass spectrometry. |
| T1 |
0-141 |
Sentence |
denotes |
Chlorination of cellulose with N-chlorosuccinimide-triphenylphosphine under homogeneous conditions in lithium chloride-N,N-dimethylacetamide. |
| T2 |
142-288 |
Sentence |
denotes |
Microcrystalline cellulose was chlorinated with N-chlorosuccinimide-triphenylphosphine under homogeneous conditions in LiCl-N,N-dimethylacetamide. |
| T3 |
289-468 |
Sentence |
denotes |
At the early stage of the reaction only replacement of the 6-hydroxyl groups with chlorine was observed, and 3-hydroxyl groups were replaced at a lower rate with Walden inversion. |
| T4 |
469-557 |
Sentence |
denotes |
The effects of reaction conditions on the extent of chlorination were studied in detail. |
| T5 |
558-739 |
Sentence |
denotes |
More than two equivalents of chlorination reagents per glucose residue were necessary to attain a high degree of substitution (ds) by chlorine, and the maximum ds attained was 1.86. |
| T6 |
740-911 |
Sentence |
denotes |
Chlorinated disaccharides were found in the hydrolyzates of chlorodeoxycelluloses hydrolyzed under mild conditions, and their structures were studied by mass spectrometry. |