PMC:7571312 / 99660-99983 JSONTXT

{"project":"LitCovid-PD-FMA-UBERON","denotations":[{"id":"T1","span":{"begin":307,"end":310},"obj":"Body_part"}],"attributes":[{"id":"A1","pred":"fma_id","subj":"T1","obj":"http://purl.org/sig/ont/fma/fma59762"}],"text":"The combined organics were washed with water (20 mL) and brine (20 mL), dried over MgSO4, filtered, and the solvents were removed in vacuo to yield the crude product, which was purified by Biotage flash chromatography, eluting with 1–3% methanol/dichloromethane to afford the title compound as a pale brown gum, 90 mg, 39%."}

{"project":"LitCovid-PD-CLO","denotations":[{"id":"T2","span":{"begin":13,"end":21},"obj":"http://purl.obolibrary.org/obo/OBI_0100026"},{"id":"T3","span":{"begin":13,"end":21},"obj":"http://purl.obolibrary.org/obo/UBERON_0000468"},{"id":"T4","span":{"begin":294,"end":295},"obj":"http://purl.obolibrary.org/obo/CLO_0001020"},{"id":"T5","span":{"begin":307,"end":310},"obj":"http://www.ebi.ac.uk/efo/EFO_0001925"}],"text":"The combined organics were washed with water (20 mL) and brine (20 mL), dried over MgSO4, filtered, and the solvents were removed in vacuo to yield the crude product, which was purified by Biotage flash chromatography, eluting with 1–3% methanol/dichloromethane to afford the title compound as a pale brown gum, 90 mg, 39%."}

{"project":"LitCovid-PD-CHEBI","denotations":[{"id":"T21849","span":{"begin":39,"end":44},"obj":"Chemical"},{"id":"T33310","span":{"begin":83,"end":88},"obj":"Chemical"},{"id":"T79743","span":{"begin":108,"end":116},"obj":"Chemical"},{"id":"T76543","span":{"begin":237,"end":245},"obj":"Chemical"},{"id":"T18868","span":{"begin":246,"end":261},"obj":"Chemical"}],"attributes":[{"id":"A19006","pred":"chebi_id","subj":"T21849","obj":"http://purl.obolibrary.org/obo/CHEBI_15377"},{"id":"A54116","pred":"chebi_id","subj":"T33310","obj":"http://purl.obolibrary.org/obo/CHEBI_32599"},{"id":"A31503","pred":"chebi_id","subj":"T79743","obj":"http://purl.obolibrary.org/obo/CHEBI_46787"},{"id":"A31489","pred":"chebi_id","subj":"T76543","obj":"http://purl.obolibrary.org/obo/CHEBI_17790"},{"id":"A57210","pred":"chebi_id","subj":"T18868","obj":"http://purl.obolibrary.org/obo/CHEBI_15767"}],"text":"The combined organics were washed with water (20 mL) and brine (20 mL), dried over MgSO4, filtered, and the solvents were removed in vacuo to yield the crude product, which was purified by Biotage flash chromatography, eluting with 1–3% methanol/dichloromethane to afford the title compound as a pale brown gum, 90 mg, 39%."}

{"project":"LitCovid-sentences","denotations":[{"id":"T561","span":{"begin":0,"end":323},"obj":"Sentence"}],"namespaces":[{"prefix":"_base","uri":"http://pubannotation.org/ontology/tao.owl#"}],"text":"The combined organics were washed with water (20 mL) and brine (20 mL), dried over MgSO4, filtered, and the solvents were removed in vacuo to yield the crude product, which was purified by Biotage flash chromatography, eluting with 1–3% methanol/dichloromethane to afford the title compound as a pale brown gum, 90 mg, 39%."}

{"project":"LitCovid-PubTator","denotations":[{"id":"1867","span":{"begin":301,"end":310},"obj":"Species"},{"id":"1869","span":{"begin":39,"end":44},"obj":"Chemical"},{"id":"1870","span":{"begin":57,"end":62},"obj":"Chemical"},{"id":"1871","span":{"begin":83,"end":88},"obj":"Chemical"},{"id":"1872","span":{"begin":237,"end":245},"obj":"Chemical"},{"id":"1873","span":{"begin":246,"end":261},"obj":"Chemical"}],"attributes":[{"id":"A1867","pred":"tao:has_database_id","subj":"1867","obj":"Tax:338536"},{"id":"A1869","pred":"tao:has_database_id","subj":"1869","obj":"MESH:D014867"},{"id":"A1870","pred":"tao:has_database_id","subj":"1870","obj":"MESH:C017082"},{"id":"A1871","pred":"tao:has_database_id","subj":"1871","obj":"MESH:D008278"},{"id":"A1872","pred":"tao:has_database_id","subj":"1872","obj":"MESH:D000432"},{"id":"A1873","pred":"tao:has_database_id","subj":"1873","obj":"MESH:D008752"}],"namespaces":[{"prefix":"Tax","uri":"https://www.ncbi.nlm.nih.gov/taxonomy/"},{"prefix":"MESH","uri":"https://id.nlm.nih.gov/mesh/"},{"prefix":"Gene","uri":"https://www.ncbi.nlm.nih.gov/gene/"},{"prefix":"CVCL","uri":"https://web.expasy.org/cellosaurus/CVCL_"}],"text":"The combined organics were washed with water (20 mL) and brine (20 mL), dried over MgSO4, filtered, and the solvents were removed in vacuo to yield the crude product, which was purified by Biotage flash chromatography, eluting with 1–3% methanol/dichloromethane to afford the title compound as a pale brown gum, 90 mg, 39%."}