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PMC:7571312 / 87085-87982 JSONTXT

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LitCovid-PD-CLO

Id Subject Object Predicate Lexical cue
T621 350-351 http://purl.obolibrary.org/obo/CLO_0001020 denotes a
T622 396-398 http://purl.obolibrary.org/obo/CL_0000453 denotes LC
T623 498-499 http://purl.obolibrary.org/obo/CLO_0001020 denotes a
T624 649-650 http://purl.obolibrary.org/obo/CLO_0001020 denotes a
T625 852-854 http://purl.obolibrary.org/obo/CLO_0007874 denotes MS
T626 889-894 http://purl.obolibrary.org/obo/CLO_0007706 denotes M + H

LitCovid-PD-CHEBI

Id Subject Object Predicate Lexical cue chebi_id
T1521 0-2 Chemical denotes N2 http://purl.obolibrary.org/obo/CHEBI_17997
T1522 36-42 Chemical denotes chloro http://purl.obolibrary.org/obo/CHEBI_47853
T1523 45-48 Chemical denotes oxo http://purl.obolibrary.org/obo/CHEBI_46629
T1524 79-85 Chemical denotes methyl http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309
T1526 86-92 Chemical denotes propyl http://purl.obolibrary.org/obo/CHEBI_26308
T1527 168-170 Chemical denotes N2 http://purl.obolibrary.org/obo/CHEBI_17997
T1528 172-191 Chemical denotes tert-butoxycarbonyl http://purl.obolibrary.org/obo/CHEBI_48502
T1529 204-210 Chemical denotes chloro http://purl.obolibrary.org/obo/CHEBI_47853
T1530 213-216 Chemical denotes oxo http://purl.obolibrary.org/obo/CHEBI_46629
T1531 247-253 Chemical denotes methyl http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309
T1533 254-260 Chemical denotes propyl http://purl.obolibrary.org/obo/CHEBI_26308
T1534 293-296 Chemical denotes Boc http://purl.obolibrary.org/obo/CHEBI_48502
T1535 396-398 Chemical denotes LC http://purl.obolibrary.org/obo/CHEBI_73582
T1536 414-418 Chemical denotes SiO2 http://purl.obolibrary.org/obo/CHEBI_30563
T1537 429-437 Chemical denotes methanol http://purl.obolibrary.org/obo/CHEBI_17790
T1538 438-448 Chemical denotes chloroform http://purl.obolibrary.org/obo/CHEBI_35255
T1539 519-521 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1540 527-531 Chemical denotes DMSO http://purl.obolibrary.org/obo/CHEBI_28262
T1541 557-559 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1542 571-573 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1543 595-597 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1544 620-622 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1545 671-673 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1546 678-680 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1547 692-694 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1548 706-708 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1549 720-722 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1550 734-736 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1551 748-750 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1552 762-764 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1553 776-778 Chemical denotes 1H http://purl.obolibrary.org/obo/CHEBI_49637
T1554 852-854 Chemical denotes MS http://purl.obolibrary.org/obo/CHEBI_73613

LitCovid-sentences

Id Subject Object Predicate Lexical cue
T506 0-110 Sentence denotes N2-(tert-Butoxycarbonyl)-N1-((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)-l-norleucinamide
T507 111-365 Sentence denotes Following the procedure described for the preparation of N2-(tert-butoxycarbonyl)-N1-((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)-l-leucinamide but substituting Boc-NorLeu-OH and making noncritical variations provided a golden syrup.
T508 366-518 Sentence denotes This material was purified by LC (100 g 230–400 SiO2, 2.5–3.5% methanol/chloroform) to afford 727 mg (42%) of the title compound as a light yellow foam.
T509 519-670 Sentence denotes 1H NMR (DMSO-d6) δ 8.45 (d, J = 8 Hz, 1H), 7.62 (s, 1H), 7.00 (d, J = 8 Hz, 1H), 4.59 (d, J = 16 Hz, 1H), 4.53 (d, J = 16 foam in a 42% isolated yield.
T510 671-897 Sentence denotes 1H Hz, 1H), 4.38 (m, 1H), 3.80 (m, 1H), 3.15 (m, 1H), 3.06 (m, 1H), 2.22 (m, 1H), 2.07 (m, 1H), 1.98 (m, 1H), 1.63–1.51 (m, 4H), 1.36 (m, 9H), 1.24 (m, 4H), 0.83 (t, J = 8 Hz, 3H); MS (ESI+) for C19H32ClN3O5m/z 418.1 (M + H)+.

LitCovid-PubTator

Id Subject Object Predicate Lexical cue tao:has_database_id
1712 293-296 Gene denotes Boc Gene:91653
1713 414-418 Chemical denotes SiO2
1714 429-437 Chemical denotes methanol MESH:D000432
1715 438-448 Chemical denotes chloroform MESH:D002725
1716 519-521 Chemical denotes 1H
1717 527-534 Chemical denotes DMSO-d6
1718 557-559 Chemical denotes 1H
1719 571-573 Chemical denotes 1H
1720 595-597 Chemical denotes 1H
1721 620-622 Chemical denotes 1H