PMC:7571312 / 81392-81749 JSONTXT

{"project":"LitCovid-PD-CLO","denotations":[{"id":"T594","span":{"begin":74,"end":75},"obj":"http://purl.obolibrary.org/obo/CLO_0001020"}],"text":", 2–5% methanol/chloroform) to afford 21 mg (9%) of the title compound as a pale tan solid. 1H NMR (400 MHz, DMSO-d6) δ 11.58 (s, 1H), 8.42 (d, J = 6.8 Hz, 1H), 7.62 (s, 1H), 7.32 (s, 1H), 7.08 (t, J = 7.7 Hz, 1H), 7.00 (d, J = 7.8 Hz, 1H), 6.49 (d, J = 7.3 Hz, 1H), 4.49–4.55 (m, 1H), 4.32–4.41 (m, 1H), 4.21–4.30 (m, 1H), 4.12 (t, J = 16.9 Hz, 1H), 3.87 ("}

{"project":"LitCovid-PD-CHEBI","denotations":[{"id":"T1252","span":{"begin":7,"end":15},"obj":"Chemical"},{"id":"T1253","span":{"begin":16,"end":26},"obj":"Chemical"},{"id":"T1254","span":{"begin":92,"end":94},"obj":"Chemical"},{"id":"T1255","span":{"begin":109,"end":113},"obj":"Chemical"},{"id":"T1256","span":{"begin":130,"end":132},"obj":"Chemical"},{"id":"T1257","span":{"begin":156,"end":158},"obj":"Chemical"},{"id":"T1258","span":{"begin":170,"end":172},"obj":"Chemical"},{"id":"T1259","span":{"begin":184,"end":186},"obj":"Chemical"},{"id":"T1260","span":{"begin":210,"end":212},"obj":"Chemical"},{"id":"T1261","span":{"begin":236,"end":238},"obj":"Chemical"},{"id":"T1262","span":{"begin":262,"end":264},"obj":"Chemical"},{"id":"T1263","span":{"begin":281,"end":283},"obj":"Chemical"},{"id":"T1264","span":{"begin":300,"end":302},"obj":"Chemical"},{"id":"T1265","span":{"begin":319,"end":321},"obj":"Chemical"},{"id":"T1266","span":{"begin":346,"end":348},"obj":"Chemical"}],"attributes":[{"id":"A1252","pred":"chebi_id","subj":"T1252","obj":"http://purl.obolibrary.org/obo/CHEBI_17790"},{"id":"A1253","pred":"chebi_id","subj":"T1253","obj":"http://purl.obolibrary.org/obo/CHEBI_35255"},{"id":"A1254","pred":"chebi_id","subj":"T1254","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1255","pred":"chebi_id","subj":"T1255","obj":"http://purl.obolibrary.org/obo/CHEBI_28262"},{"id":"A1256","pred":"chebi_id","subj":"T1256","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1257","pred":"chebi_id","subj":"T1257","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1258","pred":"chebi_id","subj":"T1258","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1259","pred":"chebi_id","subj":"T1259","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1260","pred":"chebi_id","subj":"T1260","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1261","pred":"chebi_id","subj":"T1261","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1262","pred":"chebi_id","subj":"T1262","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1263","pred":"chebi_id","subj":"T1263","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1264","pred":"chebi_id","subj":"T1264","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1265","pred":"chebi_id","subj":"T1265","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"},{"id":"A1266","pred":"chebi_id","subj":"T1266","obj":"http://purl.obolibrary.org/obo/CHEBI_49637"}],"text":", 2–5% methanol/chloroform) to afford 21 mg (9%) of the title compound as a pale tan solid. 1H NMR (400 MHz, DMSO-d6) δ 11.58 (s, 1H), 8.42 (d, J = 6.8 Hz, 1H), 7.62 (s, 1H), 7.32 (s, 1H), 7.08 (t, J = 7.7 Hz, 1H), 7.00 (d, J = 7.8 Hz, 1H), 6.49 (d, J = 7.3 Hz, 1H), 4.49–4.55 (m, 1H), 4.32–4.41 (m, 1H), 4.21–4.30 (m, 1H), 4.12 (t, J = 16.9 Hz, 1H), 3.87 ("}

{"project":"LitCovid-PubTator","denotations":[{"id":"1671","span":{"begin":7,"end":15},"obj":"Chemical"},{"id":"1672","span":{"begin":16,"end":26},"obj":"Chemical"}],"attributes":[{"id":"A1671","pred":"tao:has_database_id","subj":"1671","obj":"MESH:D000432"},{"id":"A1672","pred":"tao:has_database_id","subj":"1672","obj":"MESH:D002725"}],"namespaces":[{"prefix":"Tax","uri":"https://www.ncbi.nlm.nih.gov/taxonomy/"},{"prefix":"MESH","uri":"https://id.nlm.nih.gov/mesh/"},{"prefix":"Gene","uri":"https://www.ncbi.nlm.nih.gov/gene/"},{"prefix":"CVCL","uri":"https://web.expasy.org/cellosaurus/CVCL_"}],"text":", 2–5% methanol/chloroform) to afford 21 mg (9%) of the title compound as a pale tan solid. 1H NMR (400 MHz, DMSO-d6) δ 11.58 (s, 1H), 8.42 (d, J = 6.8 Hz, 1H), 7.62 (s, 1H), 7.32 (s, 1H), 7.08 (t, J = 7.7 Hz, 1H), 7.00 (d, J = 7.8 Hz, 1H), 6.49 (d, J = 7.3 Hz, 1H), 4.49–4.55 (m, 1H), 4.32–4.41 (m, 1H), 4.21–4.30 (m, 1H), 4.12 (t, J = 16.9 Hz, 1H), 3.87 ("}