PMC:7571312 / 77716-78786
Annnotations
LitCovid-PD-CLO
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T579 | 376-377 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
T580 | 968-970 | http://purl.obolibrary.org/obo/CLO_0007874 | denotes | MS |
T581 | 1005-1010 | http://purl.obolibrary.org/obo/CLO_0007706 | denotes | M + H |
T582 | 1037-1042 | http://purl.obolibrary.org/obo/CLO_0007706 | denotes | M + H |
LitCovid-PD-CHEBI
Id | Subject | Object | Predicate | Lexical cue | chebi_id |
---|---|---|---|---|---|
T1073 | 77-83 | Chemical | denotes | chloro | http://purl.obolibrary.org/obo/CHEBI_47853 |
T1074 | 86-89 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T1075 | 120-126 | Chemical | denotes | methyl | http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309 |
T1077 | 127-133 | Chemical | denotes | propyl | http://purl.obolibrary.org/obo/CHEBI_26308 |
T1078 | 134-139 | Chemical | denotes | amino | http://purl.obolibrary.org/obo/CHEBI_46882 |
T1079 | 140-148 | Chemical | denotes | carbonyl | http://purl.obolibrary.org/obo/CHEBI_23019 |
T1080 | 150-163 | Chemical | denotes | 3-methylbutyl | http://purl.obolibrary.org/obo/CHEBI_30359 |
T1081 | 167-174 | Chemical | denotes | methoxy | http://purl.obolibrary.org/obo/CHEBI_32772|http://purl.obolibrary.org/obo/CHEBI_44520 |
T1083 | 175-184 | Chemical | denotes | 1H-indole | http://purl.obolibrary.org/obo/CHEBI_16881 |
T1084 | 175-177 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1085 | 178-184 | Chemical | denotes | indole | http://purl.obolibrary.org/obo/CHEBI_35581 |
T1086 | 187-198 | Chemical | denotes | carboxamide | http://purl.obolibrary.org/obo/CHEBI_23004|http://purl.obolibrary.org/obo/CHEBI_37622 |
T1088 | 216-218 | Chemical | denotes | N2 | http://purl.obolibrary.org/obo/CHEBI_17997 |
T1089 | 220-239 | Chemical | denotes | tert-butoxycarbonyl | http://purl.obolibrary.org/obo/CHEBI_48502 |
T1090 | 252-258 | Chemical | denotes | chloro | http://purl.obolibrary.org/obo/CHEBI_47853 |
T1091 | 261-264 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T1092 | 295-301 | Chemical | denotes | methyl | http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309 |
T1094 | 302-308 | Chemical | denotes | propyl | http://purl.obolibrary.org/obo/CHEBI_26308 |
T1095 | 312-318 | Chemical | denotes | methyl | http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309 |
T1097 | 461-469 | Chemical | denotes | methanol | http://purl.obolibrary.org/obo/CHEBI_17790 |
T1098 | 470-480 | Chemical | denotes | chloroform | http://purl.obolibrary.org/obo/CHEBI_35255 |
T1099 | 549-551 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1100 | 566-570 | Chemical | denotes | DMSO | http://purl.obolibrary.org/obo/CHEBI_28262 |
T1101 | 599-601 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1102 | 625-627 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1103 | 651-653 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1104 | 665-667 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1105 | 691-693 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1106 | 717-719 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1107 | 743-745 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1108 | 769-771 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1109 | 788-790 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1110 | 859-861 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1111 | 878-880 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1112 | 897-899 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1113 | 930-932 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T1114 | 968-970 | Chemical | denotes | MS | http://purl.obolibrary.org/obo/CHEBI_73613 |
LitCovid-sentences
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T470 | 0-396 | Sentence | denotes | Following the procedure described for the preparation of N-((1S)-1-{[((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)amino]carbonyl}-3-methylbutyl)-4-methoxy-1H-indole-2-carboxamide but substituting N2-(tert-butoxycarbonyl)-N1-((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)-4-methyl-l-leucinamide and making noncritical variations provided a pale yellow solid. |
T471 | 397-548 | Sentence | denotes | This material was purified by Biotage MPLC (40 M column, 2–4.5% methanol/chloroform) to afford 920 g (60%) of the title compound as an off-white solid. |
T472 | 549-1070 | Sentence | denotes | 1H NMR (400 MHz, DMSO-d6) δ 11.59 (d, J = 1.8 Hz, 1H), 8.54 (d, J = 7.8 Hz, 1H), 8.45 (d, J = 8.1 Hz, 1H), 7.64 (s, 1H), 7.32 (d, J = 1.8 Hz, 1H), 7.08 (t, J = 8.0 Hz, 1H), 7.00 (d, J = 8.3 Hz, 1H), 6.49 (d, J = 7.6 Hz, 1H), 4.52–4.62 (m, 1H), 4.40–4.51 (m, 2H), 3.87 (s, 3H), 3.01–3.16 (m, 2H), 2.19–2.31 (m, 1H), 2.03–2.12 (m, 1H), 1.91–2.01 (m, 1H), 1.81 (dd, J = 14.1, 9.9 Hz, 1H), 1.54–1.72 (m, 3H), 0.93 (s, 9H); MS (ESI+) for C25H33ClN4O5m/z 505.1 (M + H)+; HRMS (ESI+) calcd for (M + H)+ 505.2212, found 505.2204. |
LitCovid-PubTator
Id | Subject | Object | Predicate | Lexical cue | tao:has_database_id |
---|---|---|---|---|---|
1638 | 461-469 | Chemical | denotes | methanol | MESH:D000432 |
1639 | 470-480 | Chemical | denotes | chloroform | MESH:D002725 |
1640 | 1014-1018 | Disease | denotes | HRMS | |
1641 | 922-928 | CellLine | denotes | 9.9 Hz | CVCL:Z676 |