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PMC:7571312 / 69744-70874
Annnotations
LitCovid-PD-CLO
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T546 | 439-440 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
T547 | 483-485 | http://purl.obolibrary.org/obo/CL_0000453 | denotes | LC |
T548 | 584-585 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
T549 | 862-864 | http://purl.obolibrary.org/obo/CLO_0053733 | denotes | 11 |
T550 | 917-919 | http://purl.obolibrary.org/obo/CLO_0007874 | denotes | MS |
T551 | 955-960 | http://purl.obolibrary.org/obo/CLO_0007706 | denotes | M + H |
LitCovid-PD-CHEBI
Id | Subject | Object | Predicate | Lexical cue | chebi_id |
---|---|---|---|---|---|
T768 | 35-41 | Chemical | denotes | leucyl | http://purl.obolibrary.org/obo/CHEBI_32630|http://purl.obolibrary.org/obo/CHEBI_37904 |
T46442 | 42-47 | Chemical | denotes | amino | http://purl.obolibrary.org/obo/CHEBI_46882 |
T40784 | 51-54 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T772 | 84-89 | Chemical | denotes | butyl | http://purl.obolibrary.org/obo/CHEBI_41264 |
T97390 | 173-175 | Chemical | denotes | N2 | http://purl.obolibrary.org/obo/CHEBI_17997 |
T774 | 177-196 | Chemical | denotes | tert-butoxycarbonyl | http://purl.obolibrary.org/obo/CHEBI_48502 |
T5508 | 209-215 | Chemical | denotes | chloro | http://purl.obolibrary.org/obo/CHEBI_47853 |
T26823 | 218-221 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T2423 | 252-258 | Chemical | denotes | methyl | http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309 |
T28917 | 259-265 | Chemical | denotes | propyl | http://purl.obolibrary.org/obo/CHEBI_26308 |
T82726 | 307-326 | Chemical | denotes | tert-butoxycarbonyl | http://purl.obolibrary.org/obo/CHEBI_48502 |
T80982 | 327-332 | Chemical | denotes | amino | http://purl.obolibrary.org/obo/CHEBI_46882 |
T782 | 336-339 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T77931 | 369-374 | Chemical | denotes | butyl | http://purl.obolibrary.org/obo/CHEBI_41264 |
T784 | 375-395 | Chemical | denotes | 2,6-dichlorobenzoate | http://purl.obolibrary.org/obo/CHEBI_48624 |
T36317 | 483-485 | Chemical | denotes | LC | http://purl.obolibrary.org/obo/CHEBI_73582 |
T3451 | 500-504 | Chemical | denotes | SiO2 | http://purl.obolibrary.org/obo/CHEBI_30563 |
T89696 | 515-523 | Chemical | denotes | methanol | http://purl.obolibrary.org/obo/CHEBI_17790 |
T41704 | 524-534 | Chemical | denotes | chloroform | http://purl.obolibrary.org/obo/CHEBI_35255 |
T50597 | 605-607 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T77382 | 613-617 | Chemical | denotes | DMSO | http://purl.obolibrary.org/obo/CHEBI_28262 |
T2563 | 643-645 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T9467 | 681-683 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T26116 | 706-708 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T59212 | 731-733 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T83656 | 745-747 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T62470 | 759-761 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T36387 | 773-775 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T99952 | 787-789 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T44278 | 801-803 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T11106 | 815-817 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T801 | 829-831 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T2297 | 917-919 | Chemical | denotes | MS | http://purl.obolibrary.org/obo/CHEBI_73613 |
T36011 | 998-1001 | Chemical | denotes | H2O | http://purl.obolibrary.org/obo/CHEBI_15377 |
T96004 | 1102-1104 | Chemical | denotes | Na | http://purl.obolibrary.org/obo/CHEBI_26708 |
LitCovid-sentences
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T430 | 0-115 | Sentence | denotes | (3S)-3-{[N-(tert-Butoxycarbonyl)-l-leucyl]amino}-2-oxo-4-[(3S)-2-oxopyrrolidin-3-yl]butyl 2,6-Dichlorobenzoate (29) |
T431 | 116-452 | Sentence | denotes | Following the procedure described for the preparation of N2-(tert-butoxycarbonyl)-N1-((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)-l-leucinamide but substituting (3S)-3-[(tert-butoxycarbonyl)amino]-2-oxo-4-[(3S)-2-oxopyrrolidin-3-yl]butyl 2,6-dichlorobenzoate and making noncritical variations provided a brown foam. |
T432 | 453-604 | Sentence | denotes | This material was purified by LC (50 g 230–400 SiO2, 2.5–3.5% methanol/chloroform) to afford 413 mg (61%) of the title compound as a light yellow foam. |
T433 | 605-963 | Sentence | denotes | 1H NMR (DMSO-d6) δ 8.47 (d, J = 8 Hz, 1H), 7.60 (m, 4H), 7.05 (d, J = 8 Hz, 1H), 5.19 (d, J = 16 Hz, 1H), 5.13 (d, J = 16 Hz, 1H), 4.47 (m, 1H), 3.95 (m, 1H), 3.16 (m, 1H), 3.08 (m, 1H), 2.27 (m, 1H), 2.10 (m, 1H), 2.03 (m, 1H), 1.65 (m, 2H), 1.47–1.37 (m, 11 H), 0.89 (d, J = 4 Hz, 3H), 0.85 (d, J = 4 Hz, 3H); MS (ESI+) for C26H35Cl2N3O7m/z 572.1 (M + H)+. |
T434 | 964-1030 | Sentence | denotes | Anal. calcd for C26H35Cl2N3O7·0.5 H2O: C, 53.70; H, 6.24; N, 7.23. |
T435 | 1031-1130 | Sentence | denotes | Found: C, 53.74; H, 6.31; N, 7.31; HRMS (ESI+) calcd for C26H35Cl2N3O7+Na 594.1744, found 594.1729. |
LitCovid-PubTator
Id | Subject | Object | Predicate | Lexical cue | tao:has_database_id |
---|---|---|---|---|---|
1519 | 500-504 | Chemical | denotes | SiO2 | |
1520 | 515-523 | Chemical | denotes | methanol | MESH:D000432 |
1521 | 524-534 | Chemical | denotes | chloroform | MESH:D002725 |
1522 | 980-993 | Chemical | denotes | C26H35Cl2N3O7 | |
1523 | 998-1001 | Chemical | denotes | H2O | |
1524 | 1003-1004 | Chemical | denotes | C | MESH:D002244 |
1525 | 1022-1023 | Chemical | denotes | N | MESH:D009584 |
1526 | 1038-1039 | Chemical | denotes | C | MESH:D002244 |
1527 | 1057-1058 | Chemical | denotes | N | MESH:D009584 |
1528 | 1088-1101 | Chemical | denotes | C26H35Cl2N3O7 | |
1529 | 1066-1070 | Disease | denotes | HRMS |