PMC:7291971 / 48622-49213
Annnotations
LitCovid-PMC-OGER-BB
| Id | Subject | Object | Predicate | Lexical cue |
|---|---|---|---|---|
| T988 | 137-146 | CHEBI:36357;CHEBI:36357 | denotes | compounds |
| T989 | 166-174 | CHEBI:75958;CHEBI:75958 | denotes | solution |
| T990 | 241-248 | CHEBI:15858;CHEBI:15858 | denotes | bromide |
| T991 | 249-256 | CHEBI:33893;CHEBI:33893 | denotes | reagent |
| T992 | 351-358 | CHEBI:60004;CHEBI:60004 | denotes | mixture |
| T993 | 397-404 | CHEBI:15377;CHEBI:15377 | denotes | aqueous |
| T994 | 505-511 | CHEBI:34683;CHEBI:34683 | denotes | Na2SO4 |
| T38632 | 137-146 | CHEBI:36357;CHEBI:36357 | denotes | compounds |
| T27381 | 166-174 | CHEBI:75958;CHEBI:75958 | denotes | solution |
| T70032 | 241-248 | CHEBI:15858;CHEBI:15858 | denotes | bromide |
| T50931 | 249-256 | CHEBI:33893;CHEBI:33893 | denotes | reagent |
| T24500 | 351-358 | CHEBI:60004;CHEBI:60004 | denotes | mixture |
| T75121 | 397-404 | CHEBI:15377;CHEBI:15377 | denotes | aqueous |
| T6076 | 505-511 | CHEBI:34683;CHEBI:34683 | denotes | Na2SO4 |
LitCovid-PubTator
| Id | Subject | Object | Predicate | Lexical cue | tao:has_database_id |
|---|---|---|---|---|---|
| 840 | 43-54 | Chemical | denotes | C26H38N13O8 | |
| 841 | 16-20 | Disease | denotes | HRMS | |
| 847 | 194-197 | Chemical | denotes | NMP | MESH:C038678 |
| 848 | 505-511 | Chemical | denotes | Na2SO4 |
LitCovid-PD-CLO
| Id | Subject | Object | Predicate | Lexical cue |
|---|---|---|---|---|
| T324 | 56-59 | http://purl.obolibrary.org/obo/CLO_0007706 | denotes | M+H |
| T325 | 164-165 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
| T326 | 453-460 | http://purl.obolibrary.org/obo/OBI_0100026 | denotes | organic |
| T327 | 453-460 | http://purl.obolibrary.org/obo/UBERON_0000468 | denotes | organic |
LitCovid-PD-CHEBI
| Id | Subject | Object | Predicate | Lexical cue | chebi_id |
|---|---|---|---|---|---|
| T915 | 166-174 | Chemical | denotes | solution | http://purl.obolibrary.org/obo/CHEBI_75958 |
| T916 | 194-197 | Chemical | denotes | NMP | http://purl.obolibrary.org/obo/CHEBI_17188|http://purl.obolibrary.org/obo/CHEBI_25608|http://purl.obolibrary.org/obo/CHEBI_7307 |
| T919 | 241-248 | Chemical | denotes | bromide | http://purl.obolibrary.org/obo/CHEBI_15858 |
| T920 | 249-256 | Chemical | denotes | reagent | http://purl.obolibrary.org/obo/CHEBI_33893 |
| T921 | 351-358 | Chemical | denotes | mixture | http://purl.obolibrary.org/obo/CHEBI_60004 |
| T922 | 376-381 | Chemical | denotes | AcOEt | http://purl.obolibrary.org/obo/CHEBI_27750 |
| T923 | 430-435 | Chemical | denotes | AcOEt | http://purl.obolibrary.org/obo/CHEBI_27750 |
| T924 | 505-511 | Chemical | denotes | Na2SO4 | http://purl.obolibrary.org/obo/CHEBI_32149 |
LitCovid-PD-GO-BP
| Id | Subject | Object | Predicate | Lexical cue |
|---|---|---|---|---|
| T50 | 124-133 | http://purl.obolibrary.org/obo/GO_0009058 | denotes | synthesis |
LitCovid-sentences
| Id | Subject | Object | Predicate | Lexical cue |
|---|---|---|---|---|
| T349 | 16-62 | Sentence | denotes | HRMS (ESI+): m/z calcd for C26H38N13O8 [M+H]+: |
| T350 | 63-79 | Sentence | denotes | 660.2961, found: |
| T351 | 80-89 | Sentence | denotes | 660.2966. |
| T352 | 91-160 | Sentence | denotes | 4.1.13 General method D for the synthesis of compounds 23, 24 and 25 |
| T353 | 161-204 | Sentence | denotes | To a solution of 20 in anhydrous NMP (conc. |
| T354 | 205-286 | Sentence | denotes | 0.03 M) was added the corresponding bromide reagent (3.00 eq) and DIEA (3.00 eq). |
| T355 | 287-392 | Sentence | denotes | After stirring for 4 h at 110 °C under microwaves, the reaction mixture was diluted with AcOEt and brine. |
| T356 | 393-542 | Sentence | denotes | The aqueous layer was extracted with AcOEt and the combined organic extracts were washed with brine, dried over Na2SO4 and concentrated under vacuum. |