PMC:7571312 / 102809-103839
Annnotations
LitCovid-PD-CLO
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T22 | 371-372 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
T23 | 522-523 | http://purl.obolibrary.org/obo/CLO_0001020 | denotes | a |
T24 | 983-985 | http://purl.obolibrary.org/obo/CLO_0007874 | denotes | MS |
T25 | 1022-1027 | http://purl.obolibrary.org/obo/CLO_0007706 | denotes | M + H |
LitCovid-PD-CHEBI
Id | Subject | Object | Predicate | Lexical cue | chebi_id |
---|---|---|---|---|---|
T85128 | 77-83 | Chemical | denotes | chloro | http://purl.obolibrary.org/obo/CHEBI_47853 |
T16482 | 86-89 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T52838 | 120-126 | Chemical | denotes | methyl | http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309 |
T7376 | 127-133 | Chemical | denotes | propyl | http://purl.obolibrary.org/obo/CHEBI_26308 |
T96266 | 134-139 | Chemical | denotes | amino | http://purl.obolibrary.org/obo/CHEBI_46882 |
T8256 | 140-148 | Chemical | denotes | carbonyl | http://purl.obolibrary.org/obo/CHEBI_23019 |
T60449 | 150-163 | Chemical | denotes | 3-methylbutyl | http://purl.obolibrary.org/obo/CHEBI_30359 |
T28806 | 167-174 | Chemical | denotes | methoxy | http://purl.obolibrary.org/obo/CHEBI_32772|http://purl.obolibrary.org/obo/CHEBI_44520 |
T20881 | 175-184 | Chemical | denotes | 1H-indole | http://purl.obolibrary.org/obo/CHEBI_16881 |
T98928 | 175-177 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T87171 | 178-184 | Chemical | denotes | indole | http://purl.obolibrary.org/obo/CHEBI_35581 |
T83064 | 187-198 | Chemical | denotes | carboxamide | http://purl.obolibrary.org/obo/CHEBI_23004|http://purl.obolibrary.org/obo/CHEBI_37622 |
T81926 | 219-238 | Chemical | denotes | tert-butoxycarbonyl | http://purl.obolibrary.org/obo/CHEBI_48502 |
T54816 | 250-256 | Chemical | denotes | chloro | http://purl.obolibrary.org/obo/CHEBI_47853 |
T52496 | 259-262 | Chemical | denotes | oxo | http://purl.obolibrary.org/obo/CHEBI_46629 |
T79162 | 293-299 | Chemical | denotes | methyl | http://purl.obolibrary.org/obo/CHEBI_32875|http://purl.obolibrary.org/obo/CHEBI_29309 |
T50557 | 300-306 | Chemical | denotes | propyl | http://purl.obolibrary.org/obo/CHEBI_26308 |
T73976 | 310-327 | Chemical | denotes | phenylalaninamide | http://purl.obolibrary.org/obo/CHEBI_21371 |
T66397 | 465-473 | Chemical | denotes | methanol | http://purl.obolibrary.org/obo/CHEBI_17790 |
T28248 | 474-489 | Chemical | denotes | dichloromethane | http://purl.obolibrary.org/obo/CHEBI_15767 |
T23370 | 550-552 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T42571 | 567-571 | Chemical | denotes | DMSO | http://purl.obolibrary.org/obo/CHEBI_28262 |
T80029 | 600-602 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T31051 | 626-628 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T39463 | 652-654 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T73098 | 666-668 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T11300 | 718-720 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T22367 | 770-772 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T29269 | 784-786 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T35866 | 810-812 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T13469 | 836-838 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T87006 | 850-852 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T56958 | 921-923 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T47490 | 940-942 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T39016 | 959-961 | Chemical | denotes | 1H | http://purl.obolibrary.org/obo/CHEBI_49637 |
T44950 | 983-985 | Chemical | denotes | MS | http://purl.obolibrary.org/obo/CHEBI_73613 |
LitCovid-sentences
Id | Subject | Object | Predicate | Lexical cue |
---|---|---|---|---|
T574 | 0-391 | Sentence | denotes | Following the procedure described for the preparation of N-((1S)-1-{[((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)amino]carbonyl}-3-methylbutyl)-4-methoxy-1H-indole-2-carboxamide but substituting N-(tert-butoxycarbonyl)-N-((1S)-3-chloro-2-oxo-1-{[(3S)-2-oxopyrrolidin-3-yl]methyl}propyl)-l-phenylalaninamide and making noncritical variations provided a crude green solid. |
T575 | 392-549 | Sentence | denotes | This material was purified by Biotage flash chromatography, eluting with methanol/dichloromethane to afford the title compound as a white solid, 300 mg, 91%. |
T576 | 550-1030 | Sentence | denotes | 1H NMR (400 MHz, DMSO-d6) δ 11.52 (d, J = 2.0 Hz, 1H), 8.68 (d, J = 7.8 Hz, 1H), 8.61 (d, J = 7.8 Hz, 1H), 7.61 (s, 1H), 7.37 (d, J = 7.1 Hz, 2H), 7.31 (d, J = 1.8 Hz, 1H), 7.26 (t, J = 7.6 Hz, 2H), 7.16 (t, J = 7.2 Hz, 1H), 7.07 (t, 1H), 6.97 (d, J = 8.1 Hz, 1H), 6.49 (d, J = 7.6 Hz, 1H), 4.68 (m, 1H), 4.38–4.49 (m, 3H), 3.88 (s, 3H), 2.97–3.17 (m, 4H), 2.20–2.32 (m, 1H), 2.02–2.14 (m, 1H), 1.93–2.02 (m, 1H), 1.52–1.69 (m, 2H); MS (APCI±) for C27H29N4O5Cl m/z 526.0 (M + H)−. |
LitCovid-PubTator
Id | Subject | Object | Predicate | Lexical cue | tao:has_database_id |
---|---|---|---|---|---|
1896 | 465-473 | Chemical | denotes | methanol | MESH:D000432 |
1897 | 474-489 | Chemical | denotes | dichloromethane | MESH:D008752 |