Method Solution Concentrations Relation Clay/Water (g/mL) Mass of Clay d001 (Å) SBET (m2/g) Observation (Pillaring Agent) Natural - - - 15.1 58 - Traditional 0.2 mol/L 1/100 3 g 17.8 234 6 days 3 0.6 mol/L 1/100 10 g 17.9 216 6 days 11 0.6 mol/L 1/100 10 g 17.6 237 60 °C, 24 h 12 1.2 mol/L 1/100 20 g 17.7 191 6 days 13 1.2 mol/L 1/100 20 g 17.5 251 60 °C, 24 h 14 1.5 mol/L 1/100 50 g 16.6 179 6 days 15 1.2 mol/L 1/100 50 g 17.6 197 6 days 16 1.2 mol/L 1/100 50 g 17.6 233 60 °C, 24 h