Method(s) # Identified # Quantified Year Reference Multiple 51 51 1971 Putnam [105] GC-MS 52 0 1976 Lawson [85] GC-MS 72 72 1978 Gates [106] GC-MS 36 36 1989 Hoffman [107] GC-MS 137 0 1990 Liebich [108] GC-MS 131 95 1991 Shoemaker [84] GC-MS 69 69 1994 Guneral [56] GC-MS 75 75 1996 Matsumoto [109] ICP-MS 33 33 2005 Goulle [110] SPE/NMR 73 0 2008 Yang [40] SPE/LC/NMR 72 0 2008 Rezzi [78] LC-MS/NMR 50 0 2008 Law [34] LC-MS 93 93 2009 Guo [111] NMR 50 50 2009 Shaykhutdinov [112] GC-MS-MS 48 48 2011 Kvitvang [113] SPE-GC-MS 79 0 2011 Silva [114] LC-MS 167 0 2011 Guo [115] NMR 42 42 2011 Saude [116] NMR/GC-MS 77 0 2012 Zhang [117] LC-MS 219 (25 listed) 0 2012 Van der Kloet [118] GC-TOF/LC-MS 261 0 2012 Cheng [119] GC-MS 258 0 2012 Roux [83] GCxGC-TOF-MS 294 0 2012 Rocha [120]